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Beilstein J. Org. Chem. 2015, 11, 2677–2688, doi:10.3762/bjoc.11.288
Graphical Abstract
Scheme 1: Synthetic route of 3·TM-βCD and 3·TM-γCD polyrotaxanes, and the non-rotaxane counterpart 3.
Figure 1: 1H NMR spectrum of the polyrotaxane 3·TM-βCD copolymer in CDCl3.
Figure 2: DSC traces on second heating scan of 3, 3·TM-βCD and 3·TM-γCD compounds.
Figure 3: Optical properties of 3·TM-γCD (dotted line), 3·TM-βCD (dashed line) and 3 (solid line) polymers: a...
Figure 4: CV of 3 (a), 3·TM-βCD (b) and 3·TM-γCD (c) in 0.1 M tetrabutylammonium perchlorate (TBAClO4)/ACN so...
Figure 5: Representative AFM images obtained over 3 × 3 µm2 areas of the non-rotaxane 3 (a), 3·TM-βCD (b) and ...